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Browsing by Author "Naether, C."

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Reversible hydration characteristics of Group VI tetrathiometalates derived from Tris(2-aminoethyl)amine

Srinivasan, B.R.; Dhuri, S.N.; Naether, C.; Bensch, W. (Thermans-2006. 2006; 267-.)

The complexes (trenH2)[MoS4]·H2O 1 and (trenH2)[WS4]·H2O 2 (tren = tris(2-aminoethylamine) were synthesized by the base promoted cation exchange method. Both complexes can be dehydrated to the corresponding anhydrous ...
Solid state synthesis and characterization of a triple chain calcium(II) coordination polymer showing two different bridging 4-nitrobenzoate coordination modes

Srinivasan, B.R.; Shetgaonkar, S.Y.; Naether, C.; Bensch, W. (Polyhedron 28(3); 2009; 534-540.)

The solid state reaction of [Ca(H2O)4(eta1-4-nba)(eta2-4-nba)] 1 (4-nba = 4-nitrobenzoate) with 2-methylimidazole (L2) at 100 degrees C results in the formation of a Ca(II) coordination polymer [Ca(H2O)(L2)(4-nba)2]n 2. ...
A spiral-like chain from a hydrogen-bonded cyclic dichloride containing a water dimer in a quaternary diammonium dichloride trihydrate

Srinivasan, B.R.; Mhalsikar, R.G.; Rane, K.S.; Naether, C.; Bensch, W. (Journal of Chemical Sciences. 119(1); 2007; 21-27.)

The reaction of benzyl chloride with tetramethylethylenediamine (tmen) results in the formation of the quaternary diammonium dichloride trihydrate (dbtmen)Cl2·3H2O 1 (dbtmen is N,N'-dibenzylN,N,N',N'-tetramethylethylenediammonium) ...
Structural characterization of sodium and potassium 3-nitrohydrogenphthalate coordination polymers

Jyai, R.N.; Naether, C.; Bensch, W.; Srinivasan, B.R. (Zeitschrift für Naturforschung B. 77(6); 2022; 433-440.)

The synthesis, crystal structures and properties of two alkali metal 3-nitrohydrogenphthalates obtained by a 1:2 reaction of M sub(2)CO sub(3) (M = K or Na) with 3-nitrophthalic acid (LH sub(2)) are reported. In the anhydrous ...
Synthesis and characterization of a mixed cationic tetrasulfidotungstate monohydrate

Srinivasan, B.R.; Mhalsikar, Rathan G.; Naether, C.; Bensch, W. (Indian Journal of Chemistry Section A-Inorganic Bio-Inorganic Physical Theoretical and Analytical Chemistry. 49(7); 2010; 891-895.)

Synthesis and structural characterization of a mixed cationic tetrasulficlotungstate monohydrate (dabcoH)(3)(NMe(4))[WS(4)](2).H(2)O (dabco = 1,4-diazabicyclo[2.2.2]octane; NMe(4) = tetramethylammonium) is described. The ...
Synthesis and characterization of bis(alkylammonium) tetrasulfidometalates

Srinivasan, B.R.; Girkar, S.V.; Naether, C.; Bensch, W. (Journal of Coordination Chemistry. 63(6); 2010; 931-942.)

The synthesis and characterization of the bis(alkylammonium) tetrasulfidometalates, (EtNH(3))(2)[MS(4)] (M = W 1, Mo 2), [BuNH(3)](2)[MS(4)] (M = W 3; Mo 4) and (Et-enH(2))[WS(4)] 1-en (Et-en = N-ethylethane-1,2-diamine), ...
Synthesis and solid state characterization of two insoluble tetrathiometalates

Srinivasan, B.R.; Dhuri, S.N.; Naether, C.; Bensch, W. (Transition Metal Chemistry. 32(1); 2007; 64-69.)

The aqueous reaction of ammonium tetrathiometalates (NH(4))(2)[MS(4)] (M = Mo or W) with (dbtmen)Br(2) center dot 2H(2)O (dbtmen = N,N'-dibenzyl-N,N,N ', N'-tetramethylethylenediammonium dication) results in the formation ...
Synthesis and structural characterization of 1-methylpiperazinediium tetrasulfidotungstate monohydrate

Srinivasan, B.R.; Naik, A.R.; Naether, C.; Bensch, W. (Indian Journal of Chemistry Section A-Inorganic Bio-Inorganic Physical Theoretical and Analytical Chemistry. 49(4); 2010; 437-441.)

The reaction of (NH(4))(2)[WS(4)] with 1-methylpiperazine results in the formation of 1-methylpiperazinediium tetrasulfidotungstate monohydrate, in good yield. (Me-pipH(2))[WS(4)].H(2)O has been characterized by elemental ...
Synthesis and structural characterization of bis(dimethylammonium) tetrasulfidometalates

Srinivasan, B.R.; Girkar, S.V.; Naether, C.; Bensch, W. (Journal of Coordination Chemistry. 62(22); 2009; 3559-3572.)

Reaction of (NH(4))(2)[MS(4)] (M = Mo, W) with aqueous dimethylamine (CH(3))(2)NH or KOH results in the formation of bis(dimethylammonium) tetrasulfidometalates [(CH(3))(2)NH(2)](2)[MS(4)] (M = W 1; Mo 2) or dipotassium ...
Synthesis and structural characterization of bis(n-propylammonium) tetrasulfidometalates

Srinivasan, B.R.; Naik, A.R.; Naether, C.; Bensch, W. (Indian Journal of Chemistry Section A-Inorganic Bio-Inorganic Physical Theoretical and Analytical Chemistry. 48(6); 2009; 769-774.)

The reaction of (NH(4))(2)[MS(4)] (M = W, Mo) with n-propylamine (CH(3)-CH(2)-CH(2)-NH(2)) results in the formation of bis(n-propylammonium) tetrasulfidometalates (CH(3)-CH(2)-CH(2)-NH(3))(2)[MS(4)] (M = W (1): Mo (2)). ...
Synthesis and structural characterization of tris(ethylenediamine)nickel(II) dichromate

Srinivasan, B.R.; Naik, A.R.; Naether, C.; Pausch, H.; Bensch, W. (Journal of Coordination Chemistry. 62(22); 2009; 3583-3591.)

The reaction of tris(ethylenediamine)nickel(II) dichloride dihydrate with potassium dichromate or potassium chromate results in the formation of mixed metallic compounds tris(ethylenediamine)nickel(II) dichromate ...
Synthesis and structural characterization of two new non-centrosymmetric tetrasulfidometalates

Srinivasan, B.R.; Dhuri, S.N.; Naik, A.R.; Naether, C.; Bensch, W. (Zeitschrift Fur Anorganische Und Allgemeine Chemie. 639(41702); 2013; 512-516.)

The synthesis and structural characterization of two new group VI tetrasulfidometalates (NH4)6[MS4]3.(hmt)4 [hmt = hexamethylenetetramine; M = W (1); M = Mo (2)] is reported. 1 and 2 are isostructural and crystallize in ...
Synthesis and structure of tris (acetylacetonato) aluminum(III)

Shirodker, M.; Borker, V.; Naether, C.; Bensch, W.; Rane, K.S. (Indian Journal of Chemistry Section A-Inorganic Bio-Inorganic Physical Theoretical and Analytical Chemistry. 49(12); 2010; 1607-1611.)

Tris(acetylacetonato)aluminium(III), [Al(C2H7O2)(3)], a precursor in vapor deposition of aluminum oxide, has been prepared starting from industrial alum, Al-2(SO4)(3).16H(2)O and characterized by chemical, IR, thermal ...
Synthesis, crystal structure and properties of hepta(ammonium) penta(1H-imidazol-3-ium) paratungstate B tetrahydrate

Srinivasan, B.R.; Kundaikar, S.A.; Morajkar, S.M.; Naether, C.; Bensch, W. (Journal of Coordination Chemistry. 74(13); 2021; 2239-2252.)

An attempted isolation of the elusive diammonium tetraoxidotungstate (NH sub(4)) sub(2)[WO sub(4)] as its imidazole (Im) adduct resulted in the serendipitous formation of hepta(ammonium) penta(1H-imidazol-3-ium) paratungstate ...
Synthesis, crystal structures and properties of three new tetrathiomolybdates with organic ammonium cations

Srinivasan, B.R.; Dhuri, S.N.; Poisot, M.; Naether, C.; Bensch, W. (Zeitschrift Fur Naturforschung Section B-A Journal of Chemical Sciences. 59(10); 2004; 1083-1092.)

Three new tetrathiomolybdates (pipH(2))[MoS4] (1), (trenH(2))[MoS4]. H2O (2) and [(prop)(4)N](2)[MoS4] (3) (pip = piperazine, tren = tris(2-aminoethyl)amine and prop = n-propyl) were synthesized and characterized by elemental ...
Synthesis, properties and structural characterization of 4-(2-ammonioethyl)piperazin-1-ium tetrasulfidotungstate hemihydrate and 1-ethylpiperazinediium tetrasulfidotungstate

Srinivasan, B.R.; Naik, A.R.; Dhuri, S.N.; Naether, C.; Bensch, W. (Polyhedron. 28(17); 2009; 3715-3722.)

The reaction of ammonium tetrasulfidotungstate with 2-piperazin-1-ylethanamine or 1-ethylpiperazine results in the formation of 4-(2-ammonioethyl)piperazin-1-ium tetrasulfidotungstate hemihydrate (C(6)H(17)N(3))[WS(4)].1/2H(2)O ...
Synthesis, properties and supramolecular structure of piperazinediium thiosulfate monohydrate

Srinivasan, B.R.; Naik, A.R.; Dhuri, S.N.; Naether, C.; Bensch, W. (Journal of Chemical Sciences. 123(1); 2011; 55-61.)

Aqueous reaction of ammonium thiosulfate with piperazine (pip) results in the formation of the title compound (pipH(2))[S2O3].H2O 1 (pipH(2) = piperazinediium) in good yield. 1 was characterized by elemental analysis, IR. ...
Synthesis, spectroscopic and X-ray structure characterization of ethylenediammonium chromate and ethylenediammonium dichromate

Srinivasan, B.R.; Dhuri, S.N.; Naether, C.; Bensch, W. (Indian Journal of Chemistry Section A-Inorganic Bio-Inorganic Physical Theoretical and Analytical Chemistry. 42; 2003; 2735-2741.)

The reaction of ethylenediammonium chloride (enH2)Cl2 with potassium chromate or dichromate in a 1:1 mole ratio results in the formation of the title complexes ethylenediammonium chromate (enH2)[CrO4] 1 and ethylenediammonium ...
Synthesis, spectroscopic, thermal and X-ray structure characterization of 1,3-propanediammonium tetrathiomolybdate and N,N,N ',N '-tetramethylethylenediammonium tetrathiomolybdate

Srinivasan, B.R.; Dhuri, S.N.; Naether, C.; Bensch, W. (Inorganica Chimica Acta. 358(2); 2005; 279-287.)

The title compounds 1,3-propanediammonium tetrathiomolybdate, (1,3-pnH(2))[MoS4], 1 and, NNN',N'-tetramethylethylenediammonium tetrathiomolybdate, (tmenH(2))[MoS4], 2, were prepared by reacting the ammonium salt of [MoS4](2-) ...
Synthesis, spectroscopy and crystal structures of chiral organic ammonium tetrathiometalates showing N-H.S and C-H.S interactions

Srinivasan, B.R.; Naik, A.R.; Naether, C.; Bensch, W. (Zeitschrift Fur Anorganische Und Allgemeine Chemie. 633(4); 2007; 582-588.)

The reaction of ammonium tetrathiometalate (NH4)2[MS4] (M = W or Mo) with the R(+) or S(-) forms of the organic amine alpha-methylbenzylamine [PhCH(CH3)NH2] results in the formation of the corresponding non-centrosymmetric ...

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