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Browsing by Author "Shetgaonkar, S.Y."

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A calcium(II) coordination polymer based on a tricyclic dicalcium-bis(2-nitrobenzoate) building block

Srinivasan, B.R.; Shetgaonkar, S.Y.; Raghavaiah, P. (Polyhedron. 28(14); 2009; 2879-2886.)

The reaction of CaCO(3) with 2-nitrobenzoic acid (2-nbaH) results in the formation of a coordination polymer, [Ca(2-nba)(2)(H(2)O)(2)](n) (1) (2-nba = 2-nitrobenzoate), which can be dehydrated to [Ca(2-nba)(2)] (2). Compound ...
A calcium(II) coordination polymer showing two different bridging 2-carbamoyl-4-nitrobenzoate coordination modes

Srinivasan, B.R.; Shetgaonkar, S.Y. (Journal of Coordination Chemistry. 63(19); 2010; 3403-3412.)

Aqueous reaction of CaCO3 with 2-carbamoyl-4-nitrobenzoic acid (2-ca-4nbaH) results in the formation of a 1-D coordination polymer [Ca(H2O)2(2-ca-4nba)2] (1), which crystallizes in the centrosymmetric triclinic space group ...
Chemistry of S-block Metal Coordination Polymers: Synthesis, Reactivity Characteristics, Spectroscopic and Structural Investigations

Shetgaonkar, S.Y.
First alkaline earth 2-carbarnoyl-4-nitrobenzoate: Synthesis and supramolecular structure

Srinivasan, B.R.; Shetgaonkar, S.Y.; Raghavaiah, P. (Indian Journal of Chemistry Section A-Inorganic Bio-Inorganic Physical Theoretical and Analytical Chemistry. 48(12); 2009; 1662-1666.)

2-Carbamoyl-4-nitrobenzoic acid (2-ca-4nbaH) -has been prepared by alkaline hydrolysis of 4-nitrophthalimide. Aqueous reaction of MgCO(3) with 2-ca-4nbaH results in the formation of [Mg(H(2)O)(6)](2-ca-4nba)(2), which ...
A new calcium(II) coordination polymer based on a mu(2)-bridging tridentate 4-nitrobenzoate

Srinivasan, B.R.; Shetgaonkar, S.Y.; Saxena, M.; Naether, C. (Indian Journal of Chemistry Section A-Inorganic Bio-Inorganic Physical Theoretical and Analytical Chemistry. 51(3); 2012; 435-443.)

Reaction of a heptacoordinated Ca(II) compound [Ca(H2O)(4)(4-nba)(2)] (4-nba = 4-nitrobenzoate) with 3,5-dimethylpyrazole (dmp) leads to the formation of an eight coordinated Ca(II) compound, [[Ca(H2O)(2)(4-nba)(2)].2dmp](n), ...
A one-dimensional barium(II) coordination polymer with a coordinated nitro group of 2-nitrobenzoate

Srinivasan, B.R.; Shetgaonkar, S.Y.; Raghavaiah, P. (Journal of Chemical Sciences. 120(2); 2008; 249-257.)

The aqueous reaction of barium carbonate with 2-nitrobenzoic acid (2-nbaH) results in the formation of a one-dimensional coordination polymer, catena-poly[[hexa(aqua)dibarium(II)]bis[(mu(2)-2-nitrobenzoate-O,O,O-NO2)(mu( ...
Preparation, crystal structures, and thermal studies of alkaline earth nitrocarboxylates

Srinivasan, B.R.; Shetgaonkar, S.Y.; Naether, C. (Zeitschrift Fur Anorganische Und Allgemeine Chemie. 637(1); 2011; 130-136.)

The preparation, crystal structures, and thermal properties of [Ca(pyr)(2)(4-nba)(2)](n)(1)(pyr = pyrazole; 4-nba = 4-nitrobenzoate) {[Ca(H2O)(2)(3-npth)].H2O}(n) (2) (3-npth = 3-nitrophthalate), [Mg(H2O)(5)(3-npth)].2H(2)O ...
Soft synthesis of a metal-organic framework based on a tribarium building block

Srinivasan, B.R.; Shetgaonkar, S.Y.; Raghavaiah, P. (Indian Journal of Chemistry Section A-Inorganic Bio-Inorganic Physical Theoretical and Analytical Chemistry. 51(8); 2012; 1064-1072.)

Reaction of MCO3 (M = Ba or Ca) with benzene-1,3,5-tricarboxylic acid (H(3)btc) in aqueous medium at room temperature affords in good yields the metal-organic framework material [Ba-3(btc)(2)(H2O)(8)].2H(2)O (1) or the ...
Solid state synthesis and characterization of a triple chain calcium(II) coordination polymer showing two different bridging 4-nitrobenzoate coordination modes

Srinivasan, B.R.; Shetgaonkar, S.Y.; Naether, C.; Bensch, W. (Polyhedron 28(3); 2009; 534-540.)

The solid state reaction of [Ca(H2O)4(eta1-4-nba)(eta2-4-nba)] 1 (4-nba = 4-nitrobenzoate) with 2-methylimidazole (L2) at 100 degrees C results in the formation of a Ca(II) coordination polymer [Ca(H2O)(L2)(4-nba)2]n 2. ...
Synthesis and characterization of calcium(II) coordination polymers based on phenylacetic acid

Srinivasan, B.R.; Shetgaonkar, S.Y.; Ghosh, N.N. (Journal of Coordination Chemistry. 64(7); 2011; 1113-1124.)

The syntheses, crystal structures, and thermal properties of the coordination polymers [Ca(H2O)2(L1)2].H2O (1) (L1 = 4-methoxyphenylacetate) and [Ca(H2O)2(L2)2].2H2O (2) (L2 = 2-chlorophenylacetate) are described. 1 and 2 ...
Synthesis and structural characterization of Bis(mu(2)-aqua)tetrakis(aqua)dilithium(i) Bis(4-nitrobenzoate)

Srinivasan, B.R.; Shetgaonkar, S.Y.; Dhavskar, K.T.; Sundar, J.K.; Natarajan, S. (Indian Journal of Chemistry Section A-Inorganic Bio-Inorganic Physical Theoretical and Analytical Chemistry. 51(4); 2012; 564-570.)

Reaction of alkali metal carbonates M2CO3 (M = Li or Na) with 4-nitrobenzoic acid (4-nbaH) results in the formation of [(H2O)(4)Li-2(mu-H2O)(2)](4-nba)(2) (4-nba = 4-nitrobenzoate) (1) and [Na(4-nba)(H2O)(3)] (2). Compounds ...
Synthesis, characterization and properties of a water-rich calcium(II)-4-nitrobenzoate

Srinivasan, B.R.; Shetgaonkar, S.Y.; Kohli, Sabeta; Rajnikant (Indian Journal of Chemistry Section A-Inorganic Bio-Inorganic Physical Theoretical and Analytical Chemistry. 49(11); 2010; 1468-1477.)

Solid state reaction of [Ca(H2O)(4)((4)-nba)(2)] (4-nba = 4-nitrobenzoate) with 2-aminopyridine (2-ap) at 100 degrees C results in the formation of an anhydrous compound, [Ca(2-ap)(4-nba)(2)], while in aqueous solution, ...
Synthesis, x-ray structure and properties of a calcium(II) coordination polymer showing mu(2)-eta(1):eta(1) and mu(3)-eta(2):eta(1) coordination modes of 4-nitrobenzoate

Srinivasan, B.R.; Shetgaonkar, S.Y.; Sawant, J.V.; Raghavaiah, P. (Polyhedron. 27(15); 2008; 3299-3305.)

The reaction of the monomeric compound [Ca(H2O)(4)(eta(1)-4-nba)(eta(2)-4-nba)] 1 (4-nba = 4-nitrobenzoate) with N-methylimidazole (N-Melm) or imidazole (Im) at 100 degrees C results in the formation of the anhydrous mixed ...

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