Ni0.5Mn0.1Zn0.4Fe2(C4H2O4)3 center dot 6N(2)H(4) precursor and Ni0.5Mn0.1Zn0.4Fe2O4 nanoparticle

Gawas, U.B.; Mojumdar, S.C.; Verenkar, V.M.S.

dc.contributor.author	Gawas, U.B.
dc.contributor.author	Mojumdar, S.C.
dc.contributor.author	Verenkar, V.M.S.
dc.date.accessioned	2015-06-03T10:10:07Z
dc.date.available	2015-06-03T10:10:07Z
dc.date.issued	2009
dc.identifier.citation	Journal of Thermal Analysis and Calorimetry. 96(1); 2009; 49-52.	en_US
dc.identifier.uri	http://dx.doi.org/10.1007/s10973-008-9836-y
dc.identifier.uri	http://irgu.unigoa.ac.in/drs/handle/unigoa/2255
dc.description.abstract	Metal carboxylato-hydrazinates are very good precursors for the synthesis of metal as well as mixed metal oxides as these, most of the times decomposes to nanosized oxides with high surface area at comparatively lower temperatures. In the present study one such novel precursor has been prepared and characterized by XRD, IR, SEM-EDS and chemical analysis. The thermal decomposition of the precursor has also been studied by isothermal, differential scanning calorimetry (DSC) and thermogravimetric analysis (TG).The precursor shows two-step dehydrazination followed by decarboxylation to form Ni0.5Mn0.1Zn0.4Fe2O4. The infrared spectra show N-N stretching frequency at 972 cm(-1) which confirms the bidentate bridging hydrazine. XRD confirms the formation of single phase Ni0.5Mn0.1Zn0.4Fe2O4.	en_US
dc.publisher	Springer Verlag (Germany); Akademiai Kiado	en_US
dc.subject	Chemistry	en_US
dc.title	Ni0.5Mn0.1Zn0.4Fe2(C4H2O4)3 center dot 6N(2)H(4) precursor and Ni0.5Mn0.1Zn0.4Fe2O4 nanoparticle	en_US
dc.type	Journal article	en_US
dc.identifier.impf	y