Synthesis and characterization of Ni(0.6)Zn(0.4)Fe(2)O(4) nano-particles obtained by auto catalytic thermal decomposition of carboxylato-hydrazinate complex

Gawas, U.B.; Verenkar, V.M.S.; Mojumdar, S.C.

dc.contributor.author	Gawas, U.B.
dc.contributor.author	Verenkar, V.M.S.
dc.contributor.author	Mojumdar, S.C.
dc.date.accessioned	2015-06-04T03:06:41Z
dc.date.available	2015-06-04T03:06:41Z
dc.date.issued	2011
dc.identifier.citation	Journal of Thermal Analysis and Calorimetry. 104(3); 2011; 879-883.	en_US
dc.identifier.uri	http://dx.doi.org/10.1007/s10973-011-1289-z
dc.identifier.uri	http://irgu.unigoa.ac.in/drs/handle/unigoa/2548
dc.description.abstract	Ni(0.6)Zn(0.4)Fe(2)O(4) nano-particles have been synthesized by self-propagating auto-combustion of nickel zinc ferrous fumarato-hydrazinate complex. The precursor complex has been characterized by chemical analysis, IR, AAS, thermal analysis and isothermal mass loss studies. The precursor on ignition undergoes self-propagating auto combustion to give Ni(0.6)Zn(0.4)Fe(2)O(4). The X-ray diffraction studies confirmed the single phase formation of nano-size 'as synthesized' Ni(0.6)Zn(0.4)Fe(2)O(4). TEM observation showed the average particle size to be 20 nm. Infrared and magnetization studies were also carried out on the 'as synthesized' Ni(0.6)Zn(0.4)Fe(2)O(4). The lower value of saturation magnetization and higher Curie temperature of 'as synthesized' ferrite also hint at the nano size nature.	en_US
dc.publisher	Springer Verlag (Germany); Akademiai Kiado	en_US
dc.subject	Chemistry	en_US
dc.title	Synthesis and characterization of Ni(0.6)Zn(0.4)Fe(2)O(4) nano-particles obtained by auto catalytic thermal decomposition of carboxylato-hydrazinate complex	en_US
dc.type	Journal article	en_US
dc.identifier.impf	y