Reinvestigation of crystal growth of thiosemicarbazide potassium chloride and thiosemicarbazide lithium chloride

Abstract

Reinvestigation of the growth of thiosemicarbazide potassium chloride crystal (1) (Chandrasekaran et al. [1]) and thiosemicarbazide lithium chloride crystal (2) (Maadeswaran et al. [2]), unambiguously confirms that compounds 1 and 2 are pure thiosemicarbazide and do not contain any alkali metal or chloride ions. In this paper we demonstrate the use of classical halide test, flame test, as well as infrared (IR) spectra for correct product characterization.